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Study on macroscopic kinetics of desorption of CO2-enriched DGA solution
- Low-Carbon Chemistry and Chemical Engineering Vol. 51, Issue 3, Pages: 68-77(2026)
- 作者机构：
1.四川大学 化学工程学院，四川 成都 610065
2.四川大学 新能源与低碳技术研究院，四川 成都 610207
- 作者简介：
- 基金信息：
DOI：10.12434/j.issn.2097-2547.20250175
CLC： TQ021.8Received：11 April 2025，
Revised：2025-05-14，
Published：25 March 2026
- 稿件说明：
移动端阅览
曾惜,唐思扬,钟山等.二甘醇胺CO2富液解吸宏观动力学研究[J].低碳化学与化工,2026,51(3):68-77.
ZENG Xi,TANG Siyang,ZHONG Shan,et al.Study on macroscopic kinetics of desorption of CO2-enriched DGA solution[J].Low-Carbon Chemistry and Chemical Engineering,2026,51(3):68-77.
曾惜,唐思扬,钟山等.二甘醇胺CO2富液解吸宏观动力学研究[J].低碳化学与化工,2026,51(3):68-77. DOI： 10.12434/j.issn.2097-2547.20250175.
ZENG Xi,TANG Siyang,ZHONG Shan,et al.Study on macroscopic kinetics of desorption of CO2-enriched DGA solution[J].Low-Carbon Chemistry and Chemical Engineering,2026,51(3):68-77. DOI： 10.12434/j.issn.2097-2547.20250175.
摘要
醇胺溶液是工业领域常用的CO
2
化学吸收剂。醇胺富液的CO
2
解吸动力学是评价醇胺类吸收剂的重要指标，研究醇胺富液的CO
2
解吸动力学和建立相应动力学模型对指导醇胺类吸收剂开发及优化具有重要意义。以富集CO
2
的5 mol/L二甘醇胺（DGA）溶液（简称“DGA富液”）为研究对象，采用连续搅拌反应装置测定其CO
2
解吸速率，同时使用反应器内旋转雷诺数（
Re
r
）和解吸温度分别作为衡量解吸过程中湍动强度和温度的状态参数，对DGA富液的CO
2
解吸动力学方程进行拟合。结果表明，与反应器内
Re
r
= 0相比，提高湍动强度（
Re
r
= 20000）可使DGA富液宏观解吸反应热降低6.21%，使表观活化能降低2.65%。在间歇解吸实验中，提高湍动强度可使DGA富液解吸CO
2
平衡负荷降低3.82%~9.16%（以转速200 r/min为基准），将解吸温度从353 K升高至372 K，可使DGA富液解吸CO
2
平衡负荷降低34.93%~39.64%。在连续解吸实验中，提高湍动强度可使CO
2
稳态解吸速率加快6.46%~79.63%（以转速200 r/min为基准），将富液解吸温度从347 K升高至376 K，可使CO
2
稳态解吸速率加快约17倍。在解吸温度为347~376 K、
Re
r
为846~7789及CO
2
负荷为1.35~2.68 mol/L的条件下，DGA富液的CO
2
解吸动力学模型为
<math id="M1"><mi>r</mi><mo>=</mo><mn mathvariant="normal">1.53</mn><mo>×</mo><msup><mrow><mn mathvariant="normal">10</mn></mrow><mrow><mn mathvariant="normal">14</mn></mrow></msup><mo>×</mo><mi mathvariant="normal">e</mi><mi mathvariant="normal">x</mi><mi mathvariant="normal">p</mi><mfenced separators="|"><mrow><mo>-</mo><mfrac><mrow><mn mathvariant="normal">2.30</mn><mo>×</mo><msup><mrow><mn mathvariant="normal">10</mn></mrow><mrow><mn mathvariant="normal">5</mn></mrow></msup><mo>-</mo><mn mathvariant="normal">1.53</mn><mo>×</mo><msup><mrow><mn mathvariant="normal">10</mn></mrow><mrow><mo>-</mo><mn mathvariant="normal">5</mn></mrow></msup><mo>×</mo><mi>R</mi><msubsup><mrow><mi>e</mi></mrow><mrow><mi mathvariant="normal">r</mi></mrow><mrow><mn mathvariant="normal">2</mn></mrow></msubsup></mrow><mrow><mn mathvariant="normal">2</mn><mi>R</mi><msub><mrow><mi>T</mi></mrow><mrow><mi mathvariant="normal">d</mi><mi mathvariant="normal">e</mi><mi mathvariant="normal">s</mi></mrow></msub></mrow></mfrac></mrow></mfenced><mo>×</mo><msup><mrow><mfenced open="[" close="]" separators="|"><mrow><msub><mrow><mi>C</mi></mrow><mrow><mi mathvariant="normal">D</mi><mi mathvariant="normal">G</mi><mi mathvariant="normal">A</mi><mo>-</mo><mi mathvariant="normal">C</mi><msub><mrow><mi mathvariant="normal">O</mi></mrow><mrow><mn mathvariant="normal">2</mn></mrow></msub></mrow></msub><mo>-</mo><mfrac><mrow><msubsup><mrow><mi>C</mi></mrow><mrow><mi mathvariant="normal">C</mi><msub><mrow><mi mathvariant="normal">O</mi></mrow><mrow><mn mathvariant="normal">2</mn></mrow></msub></mrow><mrow><mi>*</mi></mrow></msubsup><mo>×</mo><msup><mrow><msubsup><mrow><mi>C</mi></mrow><mrow><mi mathvariant="normal">D</mi><mi mathvariant="normal">G</mi><mi mathvariant="normal">A</mi></mrow><mrow><mi>*</mi></mrow></msubsup></mrow><mrow><mn mathvariant="normal">2</mn></mrow></msup></mrow><mrow><mn mathvariant="normal">6.34</mn><mo>×</mo><msup><mrow><mn mathvariant="normal">10</mn></mrow><mrow><mn mathvariant="normal">24</mn></mrow></msup><mo>×</mo><mi mathvariant="normal">e</mi><mi mathvariant="normal">x</mi><mi mathvariant="normal">p</mi><mfenced separators="|"><mrow><mo>-</mo><mfrac><mrow><mn mathvariant="normal">1.74</mn><mo>×</mo><msup><mrow><mn mathvariant="normal">10</mn></mrow><mrow><mn mathvariant="normal">5</mn></mrow></msup><mo>-</mo><mn mathvariant="normal">2.70</mn><mo>×</mo><msup><mrow><mn mathvariant="normal">10</mn></mrow><mrow><mo>-</mo><mn mathvariant="normal">5</mn></mrow></msup><mo>×</mo><mi>R</mi><msubsup><mrow><mi>e</mi></mrow><mrow><mi mathvariant="normal">r</mi></mrow><mrow><mn mathvariant="normal">2</mn></mrow></msubsup></mrow><mrow><mi>R</mi><msub><mrow><mi>T</mi></mrow><mrow><mi mathvariant="normal">d</mi><mi mathvariant="normal">e</mi><mi mathvariant="normal">s</mi></mrow></msub></mrow></mfrac></mrow></mfenced></mrow></mfrac></mrow></mfenced></mrow><mrow><mn mathvariant="normal">1.20</mn></mrow></msup></math>
https://html.publish.founderss.cn/rc-pub/api/common/picture?pictureId=102175484&type=
https://html.publish.founderss.cn/rc-pub/api/common/picture?pictureId=102175460&type=
149.60600281
18.37266731
。其中，
r
为CO
2
解吸速率，
R
为理想气体常数，
T
des
为解吸温度，
<math id="M2"><msub><mrow><mi>C</mi></mrow><mrow><mi mathvariant="normal">D</mi><mi mathvariant="normal">G</mi><mi mathvariant="normal">A</mi><mo>-</mo><mi mathvariant="normal">C</mi><msub><mrow><mi mathvariant="normal">O</mi></mrow><mrow><mn mathvariant="normal">2</mn></mrow></msub></mrow></msub></math>
https://html.publish.founderss.cn/rc-pub/api/common/picture?pictureId=102175500&type=
https://html.publish.founderss.cn/rc-pub/api/common/picture?pictureId=102175476&type=
9.99066734
3.30200005
为DGA富液CO
2
负荷，
<math id="M3"><msubsup><mrow><mi>C</mi></mrow><mrow><mi mathvariant="normal">C</mi><msub><mrow><mi mathvariant="normal">O</mi></mrow><mrow><mn mathvariant="normal">2</mn></mrow></msub></mrow><mrow><mi>*</mi></mrow></msubsup></math>
https://html.publish.founderss.cn/rc-pub/api/common/picture?pictureId=102175489&type=
https://html.publish.founderss.cn/rc-pub/api/common/picture?pictureId=102175501&type=
5.33400011
3.55599999
为DGA富液CO
2
平衡浓度，
<math id="M4"><msubsup><mrow><mi>C</mi></mrow><mrow><mi mathvariant="normal">D</mi><mi mathvariant="normal">G</mi><mi mathvariant="normal">A</mi></mrow><mrow><mi>*</mi></mrow></msubsup></math>
https://html.publish.founderss.cn/rc-pub/api/common/picture?pictureId=102175466&type=
https://html.publish.founderss.cn/rc-pub/api/common/picture?pictureId=102175490&type=
6.09600019
3.47133350
为解吸平衡时DGA浓度。
Abstract
Alcohol-amine solvents are commonly used as CO
2
chemical absorbents in industrial fields. The CO
2
desorption kinetics of alcohol-amine rich solution is an important index for evaluating alcohol-amine absorbents. Studying the CO
2
deso
rption kinetics of alcohol-amine rich solution and establishing corresponding kinetic models are of significant importance for guiding the development and optimization of alcohol-amine absorbents. Using 5 mol/L diethylene glycolamine (DGA) solution enriched with CO
2
(“DGA rich solution” for short) as the target
and a continuous stirred reactor was used to determine their CO
2
desorption rate. The rotating Reynolds number (
Re
r
) and desorption temperature in the reactor were selected as the state parameters to measure the turbulence intensity and temperature in desorption process
respectively
and the kinetic equation for CO
2
desorption of DGA rich solution was fitted. The results indicate that compared to
Re
r
= 0 in reactor
increasing the turbulence intensity (
Re
r
= 20000) can reduce the heat of macroscopic desorption reaction of DGA rich solution by 6.21% and reduce the apparent activation energy by 2.65%. In the intermittent desorption experiments
increasing the turbulence intensity can reduce the CO
2
equilibrium loading of DGA rich solution by 3.82% to 9.16% (rotational speed of 200 r/min as the reference)
and increasing the desorption temperature from 353 K to 372 K can reduce the CO
2
equilibrium loading of DGA rich solution by 34.93% to 39.64%. In the continuous desorption experiments
increasing the turbulence intensity can increase the CO
2
steady-state desorption rate from 6.46% to 79.63% (rotational speed of 200 r/min as the reference)
and increasing the solution desorption temperature from 347 K to 376 K can increase the CO
2
steady-state desorption rate by about 17-fold. The CO
2
desorption kinetics model of DGA rich solution in the desorption temperature range of 347 K to 376 K
Re
r
of 846 to 7789 and CO
2
loading of 1.35 mol/L to 2.68 mol/L is
<math id="M5"><mi>r</mi><mtext> </mtext><mo>=</mo><mtext> </mtext><mn mathvariant="normal">1.53</mn><mo>×</mo><msup><mrow><mn mathvariant="normal">10</mn></mrow><mrow><mn mathvariant="normal">14</mn></mrow></msup><mo>×</mo><mi mathvariant="normal">e</mi><mi mathvariant="normal">x</mi><mi mathvariant="normal">p</mi><mfenced separators="|"><mrow><mo>-</mo><mfrac><mrow><mn mathvariant="normal">2.30</mn><mo>×</mo><msup><mrow><mn mathvariant="normal">10</mn></mrow><mrow><mn mathvariant="normal">5</mn></mrow></msup><mo>-</mo><mn mathvariant="normal">1.53</mn><mo>×</mo><msup><mrow><mn mathvariant="normal">10</mn></mrow><mrow><mo>-</mo><mn mathvariant="normal">5</mn></mrow></msup><mo>×</mo><mi>R</mi><msubsup><mrow><mi>e</mi></mrow><mrow><mi mathvariant="normal">r</mi></mrow><mrow><mn mathvariant="normal">2</mn></mrow></msubsup></mrow><mrow><mn mathvariant="normal">2</mn><mi>R</mi><msub><mrow><mi>T</mi></mrow><mrow><mi mathvariant="normal">d</mi><mi mathvariant="normal">e</mi><mi mathvariant="normal">s</mi></mrow></msub></mrow></mfrac></mrow></mfenced><mo>×</mo><msup><mrow><mfenced open="[" close="]" separators="|"><mrow><msub><mrow><mi>C</mi></mrow><mrow><mi mathvariant="normal">D</mi><mi mathvariant="normal">G</mi><mi mathvariant="normal">A</mi><mo>-</mo><mi mathvariant="normal">C</mi><msub><mrow><mi mathvariant="normal">O</mi></mrow><mrow><mn mathvariant="normal">2</mn></mrow></msub></mrow></msub><mo>-</mo><mfrac><mrow><msubsup><mrow><mi>C</mi></mrow><mrow><mi mathvariant="normal">C</mi><msub><mrow><mi mathvariant="normal">O</mi></mrow><mrow><mn mathvariant="normal">2</mn></mrow></msub></mrow><mrow><mi>*</mi></mrow></msubsup><mo>×</mo><msup><mrow><msubsup><mrow><mi>C</mi></mrow><mrow><mi mathvariant="normal">D</mi><mi mathvariant="normal">G</mi><mi mathvariant="normal">A</mi></mrow><mrow><mi>*</mi></mrow></msubsup></mrow><mrow><mn mathvariant="normal">2</mn></mrow></msup></mrow><mrow><mn mathvariant="normal">6.34</mn><mo>×</mo><msup><mrow><mn mathvariant="normal">10</mn></mrow><mrow><mn mathvariant="normal">24</mn></mrow></msup><mo>×</mo><mi mathvariant="normal">e</mi><mi mathvariant="normal">x</mi><mi mathvariant="normal">p</mi><mfenced separators="|"><mrow><mo>-</mo><mfrac><mrow><mn mathvariant="normal">1.74</mn><mo>×</mo><msup><mrow><mn mathvariant="normal">10</mn></mrow><mrow><mn mathvariant="normal">5</mn></mrow></msup><mo>-</mo><mn mathvariant="normal">2.70</mn><mo>×</mo><msup><mrow><mn mathvariant="normal">10</mn></mrow><mrow><mo>-</mo><mn mathvariant="normal">5</mn></mrow></msup><mo>×</mo><mi>R</mi><msubsup><mrow><mi>e</mi></mrow><mrow><mi mathvariant="normal">r</mi></mrow><mrow><mn mathvariant="normal">2</mn></mrow></msubsup></mrow><mrow><mi>R</mi><msub><mrow><mi>T</mi></mrow><mrow><mi mathvariant="normal">d</mi><mi mathvariant="normal">e</mi><mi mathvariant="normal">s</mi></mrow></msub></mrow></mfrac></mrow></mfenced></mrow></mfrac></mrow></mfenced></mrow><mrow><mn mathvariant="normal">1.20</mn></mrow></msup></math>
https://html.publish.founderss.cn/rc-pub/api/common/picture?pictureId=102175513&type=
https://html.publish.founderss.cn/rc-pub/api/common/picture?pictureId=102175467&type=
137.92199707
18.28800011
. Among them
r
is the CO
2
desorption rate
R
is the ideal gas constant
T
des
is the desorption temperature
<math id="M6"><msub><mrow><mi>C</mi></mrow><mrow><mi mathvariant="normal">D</mi><mi mathvariant="normal">G</mi><mi mathvariant="normal">A</mi><mo>-</mo><mi mathvariant="normal">C</mi><msub><mrow><mi mathvariant="normal">O</mi></mrow><mrow><mn mathvariant="normal">2</mn></mrow></msub></mrow></msub></math>
https://html.publish.founderss.cn/rc-pub/api/common/picture?pictureId=102175515&type=
https://html.publish.founderss.cn/rc-pub/api/common/picture?pictureId=102175514&type=
10.32933331
3.30200005
is the CO
2
loading in DGA rich solution
<math id="M7"><msubsup><mrow><mi>C</mi></mrow><mrow><mi mathvariant="normal">C</mi><msub><mrow><mi mathvariant="normal">O</mi></mrow><mrow><mn mathvariant="normal">2</mn></mrow></msub></mrow><mrow><mi>*</mi></mrow></msubsup></math>
https://html.publish.founderss.cn/rc-pub/api/common/picture?pictureId=102175517&type=
https://html.publish.founderss.cn/rc-pub/api/common/picture?pictureId=102175530&type=
5.41866684
3.72533321
is the CO
2
equilibrium concentration in rich DGA solution
<math id="M8"><msubsup><mrow><mi>C</mi></mrow><mrow><mi mathvariant="normal">D</mi><mi mathvariant="normal">G</mi><mi mathvariant="normal">A</mi></mrow><mrow><mi>*</mi></mrow></msubsup></math>
https://html.publish.founderss.cn/rc-pub/api/common/picture?pictureId=102175533&type=
https://html.publish.founderss.cn/rc-pub/api/common/picture?pictureId=102175518&type=
6.18066692
3.30200005
is the concentration of DGA at desorption equilibrium.
关键词
Keywords
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